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GC?GC is a technique that employs two columns with orthogonal properties operating in tandem, where cryogenic slices collected from a first column (GC1) in few second intervals (2'8 sec), or modulation periods, are quickly released and separated rapidly within the modulation period on a second fast column (GC2) 37, 38. GC?GC coupled to molecular MS systems, such as quadrupole MS and time-of-flight-MS (TOF-MS) benefit from having a third degree of separation is the unique m/z spectra of different compounds. In contrast, IRMS measures only CO 2 gas resulting from the on-line combustion of the analytes, much like an FID detector, and cannot differentiate one molecule from another apart from retention times, best weight loss supplement com. Moreover, for GC?GC coupled to molecular MS, mass spectra of the GC2 separated peaks within a given GC1 slice are all structurally meaningful. A particular need is to understand animal communication, best weight loss supplement com.
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